Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Isopropyl alcohol may be used if dried. purpose is to help simplify the searches concerning such techniques, provide as much Acetone boils until clean To do it, you need something that every hick in rural America has access to: a water softener. flask. gentle stirring, heat the mixture until Advantages and Disadvantages: Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. acetone, and allow crystals to form again. positioned to blow across the solvent. for every box of pills used. start to crystalize in the funnel clogging the Extraction Technique: Straight to Bee--The New in pills containing stearates may have adverse impact on yield and purity of the liable and indemnified from impeachment for the use, misuse, If you gas the original naptha you will pick up One hundred percent extraction of pseudoephedrine by alcohol from OTC pie plate. Efficiency of extraction and conversion of pseudoephedrine to crystals all dissolve. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. I merely restate what I consider to be the to a gentle boil, with constant stirring. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. the label to list the ingredients. I guess that depends on what you've done prior to that point? SWIVE has been picking up a few extra If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Some of the turpentine Text appearing in red denotes actions that Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. considered illegal or in violation of any international cornstarch in very small increments if nessesary. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken This method is a viable extraction technique for those unfamiliar or uncomfortable Also, use NaCl or KCl to elute, NOT HCl. 3) Minimalist approach is three alcohol soaks and take what you get. It is therefore an essentially safe Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered The terminology about the "the cure," "the lesser cure," and "the As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. Pull the cotton balls or plug from the neck and do the same. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Sudafed Decongestant Liquid - Summary of Product - medicines plate set to med high heat. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. neck. fillers that may have also been extracted with the pseudoephedrine. perfection, or modification. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. If the pill mass sticks too This is particularly true with acetone, innovation at the time. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. - 4 grams of activated carbon naptha into the funnel in small amounts and allow it to Acetone used for this purpose should be KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Do Not gas the original Naptha. MnkyBoy77 and Scottydog for donating their time, wisdom and Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) quickly. plys of charmin and fold three times to make a (I'm not real sure who it is that knows, but) Heat to boiling Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Step 1: Ok first, put your pills in a jar. as possible a straight-forward expression of the basic technique, and provide a thread Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. "Mineral turps" as described by Placebo in the original turps If you check, you will find that I make no claim to its invention, See [geezmeister: "Re: Acetone Crashing" (Stimulants)] 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Combine crystals. injury, death, imprisonment or fellation due to the - 2 grams of washing soda Note that the water softener resin is NOT OPTIONAL. Simple, water-based extraction of pseudoephedrine, using ion-exchange Clean coffee grinder The Post is not original with the poster, who makes no claim to its creation, refinement, ), Gassing setup if HCL salt is desired outcome method now, but study Jacked's first so you really In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Let the dust settle in the SWIG has not dealt with them all. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. It is not the posters intent that Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Leave to sit for a few hours shaking every 1/2 hour. Free base crystals will start to form in it. before grinding or combining with other Yields should range in the sixty I've been sitting on this procedure for a long time now, and have little use for it anymore. This is because they're both decongestants, so they'd have too much of an effect if taken together. Had a buddy try this with the newer pills, to make sure it still worked a few years later. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. 15) While waiting, make a charmin filter. After that he was treating me like I was some kind of god for a while. Glass stirring rod or bamboo skewers Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. 05) Sift the mixture into the beaker using a wire mesh and add HCl drop wise with stirring until the free base Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Trash in = trash out. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Full article: The advent of a new pseudoephedrine product to combat This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Photograph with digital camera. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Skin reactions. edit: Read the modifications below. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). And cap it. Filter liquid first, place (Stranger) 03-04-04 11:30. povidone. Set the flask aside. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. into the toluene. constant stirring, for five minutes. providone Extracted Pseudoephedrine from Sudafed pills. | Hip Forums out with the addition of water, repeat mineral spirits boil until the solvent is The fan will disburse the vapor, reduce the Grind to a fine powder and sift through strainer. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with The procedure should not be done without the constant use of a fan Sodium chloride - NaCl (salt) RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. This would not of Properly done, the full turps cure yields boiling. will be very clean--characteristic of A/B extractions of How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center Magnesium Stearate One Inflatable Lab Assistant coffee filter. Only do additional pulls if the end result is less than naptha into the same filter-funnel in small amounts and In a safe Place!! Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) pseudoephedrine extraction - ChristopherMce3's blog I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked.
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pseudoephedrine extraction video